The synthesis and spectral characterization of novel nitrodiene compounds from thiols
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, vol.191, no.1, pp.9-15, 2016 (SCI-Expanded, Scopus)
- Publication Type: Article / Article
- Volume: 191 Issue: 1
- Publication Date: 2016
- Doi Number: 10.1080/10426507.2015.1049742
- Journal Name: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
- Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
- Page Numbers: pp.9-15
- Istanbul University Affiliated: Yes
Abstract
Novel S-, S,S- and S,O-substituted nitrodiene compounds were synthesized from the reactions of 2-nitro-pentachloro-1,3-butadiene (1) and various thiols in different solvent media. The N,S-substituted nitrodienes also were achieved by the reactions of S-substituted nitrodienes with using morpholine, piperidine and piperazine derivatives. All of the new compounds were characterized by elemental analysis, UV-VIS, FT-IR, H-1-NMR, NMR and mass spectroscopy.