The synthesis and spectral characterization of novel nitrodiene compounds from thiols


Ibis C., Ozkok F.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, vol.191, no.1, pp.9-15, 2016 (Journal Indexed in SCI) identifier identifier

  • Publication Type: Article / Article
  • Volume: 191 Issue: 1
  • Publication Date: 2016
  • Doi Number: 10.1080/10426507.2015.1049742
  • Title of Journal : PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
  • Page Numbers: pp.9-15

Abstract

Novel S-, S,S- and S,O-substituted nitrodiene compounds were synthesized from the reactions of 2-nitro-pentachloro-1,3-butadiene (1) and various thiols in different solvent media. The N,S-substituted nitrodienes also were achieved by the reactions of S-substituted nitrodienes with using morpholine, piperidine and piperazine derivatives. All of the new compounds were characterized by elemental analysis, UV-VIS, FT-IR, H-1-NMR, NMR and mass spectroscopy.