Synthesis and spectral properties of novel thiadiazolotriazinone derivatives

Gurbuz D., Tanyolac S.

JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, vol.77, no.7, pp.867-871, 2012 (SCI-Expanded) identifier identifier identifier

  • Publication Type: Article / Article
  • Volume: 77 Issue: 7
  • Publication Date: 2012
  • Doi Number: 10.2298/jsc110930217g
  • Journal Name: JOURNAL OF THE SERBIAN CHEMICAL SOCIETY
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.867-871
  • Istanbul University Affiliated: Yes

Abstract

A series of new 7-substitued-4H-1,3,4-thiadiazolo[2,3-c][1,2,4]-triazin-4-ones were synthesized in good yields by the reaction of 4-amino-3-mercapto-1,2,4-triazin-5(4H)-one with various aromatic carboxylic acids in the presence of phosphorus oxychloride. All the synthesized compounds were confirmed by FT-IR, NMR (H-1 and C-13) and ESI-MS spectroscopic techniques and analytical methods.