Zirconium titanate synthesis by diethanol amine based sol-gel route


Koc S. N.

JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, cilt.38, ss.277-281, 2006 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 38 Konu: 3
  • Basım Tarihi: 2006
  • Doi Numarası: 10.1007/s10971-006-6728-0
  • Dergi Adı: JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • Sayfa Sayıları: ss.277-281

Özet

ZrTiO4 powder are synthesized by a modified sol-gel route via bimetallic diethanol amine complex of zirconium and titanium alkoxides. Samples are cured at 140 degrees C and calcined between 500-800 degrees C. Powders are characterized with XRD, TGA, DTA, SEM and TEM methods. The ZrTiO4 powders are obtained at 650 degrees C from the amorphous form. No identified peaks can be attibuted to other phases, namely, zirconia and titania are not observed.