New N,S-derivatives of nitrodienes from thioallyl- and thiodibromopropyl nitrodienes


Ibis C. , Onul N.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, cilt.181, ss.2411-2417, 2006 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 181 Konu: 10
  • Basım Tarihi: 2006
  • Doi Numarası: 10.1080/10426500600695229
  • Dergi Adı: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
  • Sayfa Sayıları: ss.2411-2417

Özet

Compound 3 and 5a,b were obtained from the reaction of 1,3,4,4-tetrachloro-1-thioallyl-2-nitro-1,3-butadiene (1) with thiomorpholine (2) and piperazine derivatives 4a,b in dichloromethane. The reaction of compound 1 and bromine gave compound 6. Compounds 8 and 10 were obtained from the reaction of 6 with 1-(diphenylmethyl)piperazine (7) and piperidine (9) in dichloromethane. The derivative 13 was synthesized from the reaction of 4-bromo-1,1,3,4-tetrachloro-2nitro-1,3-butadiene (11) and allylmercaptane (12). Compounds 15 and 16a, b were obtained from the reaction of 1-allyl-4-bromo-1,3,4-trichloro-2-nitro-1,3-butadiene (13) with morpholine (14) and the piperazine derivatives 16a,b, in dichloromethane, respectively.