N,S-substituted nitrodienes from naphthylthiosubstituted nitrodienes and S-, S,S-substituted dienes from hexachloro-1,3-butadiene

Ibis, Cemil; Gokmen, Zeliha

doi:10.1080/10426500601093838

N,S-substituted nitrodienes from naphthylthiosubstituted nitrodienes and S-, S,S-substituted dienes from hexachloro-1,3-butadiene

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Ibis C., Gokmen Z.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, vol.182, no.5, pp.1053-1059, 2007 (SCI-Expanded)

Publication Type: Article / Article
Volume: 182 Issue: 5
Publication Date: 2007
Doi Number: 10.1080/10426500601093838
Journal Name: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Page Numbers: pp.1053-1059
Istanbul University Affiliated: Yes

Abstract

Mono(thio)substituted dienes 1 gave compounds 3a-c, 7, 9, and 11 on reaction with pipe-razine derivatives in dry ether. N,S-substituted nitrodiene 5 was obtained from the reaction of 1 with 1,4-dioxospriol 4. Hexachlorobutadiene 12 in a water-ethanol mixture in the presence of sodium hydroxide reacted with ethyleneglycol bismercaptoacetate 13 to give thiosubstituted thioethers 14 and 15.