Effect of sonication time on the synthesis of the CdS nanoparticle based multiwall carbon nanotube - maleic anhydride-1-octene nanocomposites


Malikov E. Y. , Altay M. , AKPEROV O. H. , Muradov M. B. , Eyvazova G. M. , Kukovecz A., ...Daha Fazla

FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES, cilt.26, ss.255-262, 2018 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 26 Konu: 5
  • Basım Tarihi: 2018
  • Doi Numarası: 10.1080/1536383x.2018.1432602
  • Dergi Adı: FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
  • Sayfa Sayıları: ss.255-262

Özet

Effect of sonication time on the synthesis of the CdS nanoparticles within the matrix obtained through the covalent functionalization of multiwall carbon nanotube (MWCNT) with maleic anhydride (MA) - 1-octene copolymer was investigated. Cadmium chloride and thiourea were used as the raw materials. MWCNTs used for the matrix were synthesized by Catalytic Chemical Vapor Deposition using Fe-Co/Al2O3 as the catalyst. The obtained nanostructures were characterized by FTIR, XRD, Raman spectroscopy, TEM, SEM, TG and UV-Vis spectroscopy. Electrophysical properties of the polymer nanocomposites obtained using different periods of time for sonication were comparably investigated. The average CdS particle diameter was between 3.9-7.9nm as confirmed independently by TEM and XRD. UV-Vis spectroscopy revealed that the obtained nanostructures are appropriate base materials for making optical devices.