Effect of sonication time on the synthesis of the CdS nanoparticle based multiwall carbon nanotube - maleic anhydride-1-octene nanocomposites

Malikov, Elvin; Altay, Melek; AKPEROV, Oktay; Muradov, Mustafa; Eyvazova, Goncha; Kukovecz, Akos; Konya, Zoltan

doi:10.1080/1536383x.2018.1432602

Effect of sonication time on the synthesis of the CdS nanoparticle based multiwall carbon nanotube - maleic anhydride-1-octene nanocomposites

Atıf İçin Kopyala

Malikov E. Y., Altay M., AKPEROV O. H., Muradov M. B., Eyvazova G. M., Kukovecz A., ...Daha Fazla

FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES, cilt.26, sa.5, ss.255-262, 2018 (SCI-Expanded)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 26 Sayı: 5
Basım Tarihi: 2018
Doi Numarası: 10.1080/1536383x.2018.1432602
Dergi Adı: FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.255-262
İstanbul Üniversitesi Adresli: Evet

Özet

Effect of sonication time on the synthesis of the CdS nanoparticles within the matrix obtained through the covalent functionalization of multiwall carbon nanotube (MWCNT) with maleic anhydride (MA) - 1-octene copolymer was investigated. Cadmium chloride and thiourea were used as the raw materials. MWCNTs used for the matrix were synthesized by Catalytic Chemical Vapor Deposition using Fe-Co/Al2O3 as the catalyst. The obtained nanostructures were characterized by FTIR, XRD, Raman spectroscopy, TEM, SEM, TG and UV-Vis spectroscopy. Electrophysical properties of the polymer nanocomposites obtained using different periods of time for sonication were comparably investigated. The average CdS particle diameter was between 3.9-7.9nm as confirmed independently by TEM and XRD. UV-Vis spectroscopy revealed that the obtained nanostructures are appropriate base materials for making optical devices.